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1,3-Bis[4-(dimethylamino)benzyl]-4,5,6,7-tetrahydro-1H-1,3-diazepan-2-ium chloride

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Author(s): Hakan Arslan | Don VanDerveer | Yetkin Gök | smail Özdemir | Bekir Çetinkaya

Journal: Acta Crystallographica Section E
ISSN 1600-5368

Volume: 65;
Issue: 1;
Start page: o109;
Date: 2009;
Original page

ABSTRACT
The title N-heterocyclic carbene derivative, C23H33N4+·Cl−, has been synthesized and characterized by elemental analysis, 1H and 13C NMR, IR spectroscopy and a single-crystal X-ray diffraction study. Ions of the title compound are linked by three C—H...Cl interactions. The seven-membered 1,3-diazepane ring has a form intermediate between twist-chair and twist-boat.

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