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3-(Piperidin-1-ium-1-yl)-6-azoniaspiro[5.5]undecane dibromide monohydrate

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Author(s): Jorge Gonzalez | Roberto Atilano-Coral | Ana Lilia Peraza-Campos | David Ortegón-Reyna | Eleuterio Álvarez

Journal: Acta Crystallographica Section E
ISSN 1600-5368

Volume: 67;
Issue: 6;
Start page: o1308;
Date: 2011;
Original page

ABSTRACT
The title compound, C15H30N22+·2Br−·H2O, was synthesized by reaction of 4-piperidinopiperidine with dibromopentane. The dication is built up from three linked piperidine rings, two of which have one quaternary N atom in common (azoniaspiro), whereas the third is N—C bonded to the azoniaspiro system and protonated on the N atom (piperidinium). All three piperidine rings adopt chair conformations. The crystal structure features O—H...Br and N—H...Br hydrogen bonds.

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