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Bis(μ-methanolato-κ2O:O)bis{[4-bromo-N′-(1-methyl-3-oxidobut-2-en-1-ylidene-κO)benzohydrazidato-κ2N′,O]oxidovanadium(V)}

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Author(s): Hon Wee Wong | Kong Mun Lo | Seik Weng Ng

Journal: Acta Crystallographica Section E
ISSN 1600-5368

Volume: 67;
Issue: 7;
Start page: m902;
Date: 2011;
Original page

ABSTRACT
The dinuclear compound, [V2(C12H11BrN2O2)2(CH3O)2O2], lies on a center of inversion. The doubly-deprotonated Schiff base O,N,O′-chelates to the VV atom; two metal atoms are bridged by the methoxide units. The coordination geometry is a distorted octahedron. Weak intermolecular C—H...N hydrogen bonding is present in the crystal structure. The bromophenyl unit is disordered over two positions, with the major component being in a 0.909 (6) proportion.
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