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(Cy2NH2O2CPh)3(SnCl4)2 AND (SnBu2)4(O2CPh)16Cl6(OH)2(Cy2NH2)16: SYNTHESIS AND SPECTROSCOPIC CHARACTERIZATION

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Author(s): Dinora De Barros | Libasse Diop | Bernard Mahieu

Journal: Scientific Study & Research. Chemistry & Chemical Engineering, Biotechnology, Food Industry
ISSN 1582-540X

Volume: 12;
Issue: 3;
Start page: 243;
Date: 2011;
Original page

Keywords: benzoate | IR | Mössbauer | monomer or oligomeric structures | SnCl4 | SnBu2 residue

ABSTRACT
The two title compounds have been synthesized, their IR and Mössbauer studies carried out. The structures are discrete and contain mono- and bidentate PhCO2-, the environment around the tin (IV) centre being octahedral (in SnCl4 adduct), trapezoidal bipyramidal (in the SnBu2 residue containing derivative). A tetranuclear monomeric or an oligomeric structure is suggested in the tetranuclear SnBu2 residue containing derivative.
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