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Effective Analysis of Dicyclanil in Lamb and Chicken Muscle using HPLCUV/Vis and LC/MS/MS

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Author(s): ByungJu Kim | Seung-Woon Myung

Journal: Mass Spectrometry Letters
ISSN 2233-4203

Volume: 2;
Issue: 2;
Start page: 45;
Date: 2011;

Keywords: Dicyclanil | Lamb | Chicken | Veterinary Drugs | HPLC | LC/MS/MS

ABSTRACT
The authors describe a method for monitoring dicyclanil levels in lamb and chicken muscle tissues. The devised procedureinvolves dicyclanyl extraction by SPE and its detection HPLC-UV/Vis and LC/MS/MS. The method was found to haveLOD and LOQ values of 0.02 mg kg−1 and 0.05~0.06 mg kg−1, respectively. The intraday precision and an accuracy of spikedsamples were found to have 2.3~10.4 RSD% and 80.9~105.7%, respectively.
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