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Síntesis y caracterización espectroscópica del cloruro de oleoilo

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Author(s): Alfonso Rivas-Gil | Cristóbal Lárez V. | Alí Bahsas B.

Journal: Avances en Química
ISSN 1856-5301

Volume: 2;
Issue: 1;
Start page: 15;
Date: 2007;
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Keywords: oleoyl chloride | oleic acid | 1HCOSY | HSQC | HMQC

ABSTRACT
Oleoyl chloride was synthetized using a recently distilled at reduced pressure oleic acid and thionyl chloride as starting materials. Acyl halide was vacuum distilled and later on characterized by FTIR, 1H-RMN and 13CRMN spectroscopy. Additional experiments of 1H-COSY, HSQC and HMQC were carried out, which allowed to assign unquestionably the structure of the synthesized material.
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