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Tetrakis[tris(2,2′-bi-1H-benzimidazole)nickel(II)] bis(phosphate) sulfate

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Author(s): Chun-Sheng Ling | Lin Yan

Journal: Acta Crystallographica Section E
ISSN 1600-5368

Volume: 64;
Issue: 11;
Start page: m1399;
Date: 2008;
Original page

ABSTRACT
The title compound, [Ni(C14H10N4)3]4(PO4)2(SO4), consists of [Ni(C14H10N4)3]2+ complex cations (.3. symmetry) and disordered anions ({overline 4} symmetry) with occupancy factors of two-thirds for PO43āˆ’ and one-third for SO42āˆ’. The Ni2+ centre is chelated by three bidentate 2,2ā€²-bi-1H-benzimidazole molecules in a distorted octahedral coordination. Nā€”H...O hydrogen bonds consolidate the building units into a framework structure.
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