Author(s): Mohd Rashid | Asif Husain | Ravinesh Mishra | Niyaz Ahmed | Nadeem Ahmed Siddique
Journal: Molbank
ISSN 1422-8599
Volume: 2012;
Issue: 3;
Start page: M766;
Date: 2012;
Original page
Keywords: Benzimidazole | oxadiazole | trichloroacetic acid
ABSTRACT
The title compound, 1-(1H-benzimidazol-2-yl)-3-[5-(trichloromethyl)-1,3,4-oxadiazol-2-yl]propan-1-one (2) was synthesized successfully from 4-(1H-benzimidazol-2-yl)-4-oxobutanehydrazide (1) under microwave irradiation in good yield by reacting with trichloroacetic acid, and the structure of title compound was confirmed on the basis of IR, 1H-NMR, 13C-NMR, MS and CHN analyses results.
Journal: Molbank
ISSN 1422-8599
Volume: 2012;
Issue: 3;
Start page: M766;
Date: 2012;
Original page
Keywords: Benzimidazole | oxadiazole | trichloroacetic acid
ABSTRACT
The title compound, 1-(1H-benzimidazol-2-yl)-3-[5-(trichloromethyl)-1,3,4-oxadiazol-2-yl]propan-1-one (2) was synthesized successfully from 4-(1H-benzimidazol-2-yl)-4-oxobutanehydrazide (1) under microwave irradiation in good yield by reacting with trichloroacetic acid, and the structure of title compound was confirmed on the basis of IR, 1H-NMR, 13C-NMR, MS and CHN analyses results.