Author(s): Shimoga D. Ganesh | Karkala V. Pai | Mahadevappa Y. Karidurganavar
Journal: Molbank
ISSN 1422-8599
Volume: 2013;
Issue: 1;
Start page: M796;
Date: 2013;
Original page
Keywords: Diels-Alder reaction | benzoquinone | triptycene
ABSTRACT
Diels Alder reaction of 4-bromophenylquinone (Br-PQ) with anthracene, followed by reduction affords the desired 4'-bromophenyl triptycene-2,5-diol (T-Br-PH). The described synthesis represents a simple and efficient method for the construction of a triptycene ring with a bromophenyl pendant. The intermediate and the final compound (T-Br-PH) have been characterized by elemental analysis, NMR, and LCMS techniques.
Journal: Molbank
ISSN 1422-8599
Volume: 2013;
Issue: 1;
Start page: M796;
Date: 2013;
Original page
Keywords: Diels-Alder reaction | benzoquinone | triptycene
ABSTRACT
Diels Alder reaction of 4-bromophenylquinone (Br-PQ) with anthracene, followed by reduction affords the desired 4'-bromophenyl triptycene-2,5-diol (T-Br-PH). The described synthesis represents a simple and efficient method for the construction of a triptycene ring with a bromophenyl pendant. The intermediate and the final compound (T-Br-PH) have been characterized by elemental analysis, NMR, and LCMS techniques.