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Improvement of the mechanical properties of spark plasma sintered hap bioceramics by decreasing the grain size and by adding multi-walled carbon nanotubes

Author(s): Veljović Đ. | Vuković G. | Steins I. | Palcevskis E. | Uskoković P.S. | Petrović R. | Janaćković Đ.

Journal: Science of Sintering
ISSN 0350-820X

Volume: 45;
Issue: 2;
Start page: 233;
Date: 2013;
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Keywords: hydroxyapatite | carbon nanotubes | grain size | nanocomposite | mechanical properties

Composites based on HAP and oxidized multi-walled carbon nanotubes (o-MWCNT) and monophase HAP materials were processed by spark plasma sintering. Starting from stoichiometric nano-sized HAP powder, monophase bioceramics were obtained with a density close to the theoretical one and with an average grain size of several hundred nanometers to micron dimensions. It was shown that decreasing the sintering temperature resulted in a decrease of the grain size, which affected an increase in the fracture toughness and hardness. The fracture toughness of an HAP/ o-MWCNT bioceramic processed at 900°C for only 5 min was 30 % higher than that of monophase HAP materials obtained under the same conditions. The addition of MWCNT during SPS processing of HAP materials caused a decrease in the grain size to the nano-dimension, which was one of the reasons for the improved mechanical properties. [Projekat Ministarstva nauke Republike Srbije, br. III45019 i FP7-REGPOT-2009-1 NANOTECH FTM, Grant Agreement Number: 245916]
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