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SYNTHESIS OF NOVEL 2,10-DICHORO-12-TRICHLOROMETHYL-6-SUBSTITUTED XANTHATO-12H-DIBENZO[d,g] [1,3,2] DIOXAPHOSPHOCIN 6-SULFIDES

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Author(s): B. Siva Kumar | M. Kasturaiah | C. Suresh Reddy

Journal: International Journal of Chemical Sciences and Research
ISSN 2249-0329

Volume: 01;
Issue: 04;
Start page: 29;
Date: 2011;
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Keywords: Dibenzodioxaphosphocin monochloride | 4-Dimethylaminopyridine | dioxa-phosphocin 6 –sulfide | Xanthates

ABSTRACT
New eight-membered phosphorous heterocyclic compounds such as 2,10 – dichloro – 12 – trichloromethyl - 6 – substituted xanthato – 12H – dibenzo[d,g] [1,3,2] dioxaphosphocin 6–sulfides were synthesized by reacting equimolar quantities of alcohols, carbondisulfide and 2,6,10-trichloromethyl-12H–dibenzo[d,g] [1,3,2] dioxaphosphocin 6 – sulfide(1) in the presence of dimethylaminopyridene(DMAP). The structures of the products were confirmed by analytical and IR, 1H, 13C, 31P, Mass spectral data and they were tested for their antimicrobial activity.

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