Author(s): Afsaneh Zonouzi | Roghieh Mirzazadeh | Seik Weng Ng
Journal: Molbank
ISSN 1422-8599
Volume: 2012;
Issue: 3;
Start page: M775;
Date: 2012;
Original page
Keywords: fully substituted phenol | fluorescence | one-pot reaction | malononitrile | dimethyl acetylenedicarboxylate | keto-enol tautomerization
ABSTRACT
A novel synthesis of a fully substituted fluorescent phenol by a one-pot reaction of dimethyl acetylendicarboxylate and malononitrile in the presence of catalysts has been developed. The structure of the synthesized compound was assigned on the basis of its elemental analysis, 1H-NMR, 13C-NMR, IR, mass spectral and X-ray data. The photophysical data of the new compound are reported.
Journal: Molbank
ISSN 1422-8599
Volume: 2012;
Issue: 3;
Start page: M775;
Date: 2012;
Original page
Keywords: fully substituted phenol | fluorescence | one-pot reaction | malononitrile | dimethyl acetylenedicarboxylate | keto-enol tautomerization
ABSTRACT
A novel synthesis of a fully substituted fluorescent phenol by a one-pot reaction of dimethyl acetylendicarboxylate and malononitrile in the presence of catalysts has been developed. The structure of the synthesized compound was assigned on the basis of its elemental analysis, 1H-NMR, 13C-NMR, IR, mass spectral and X-ray data. The photophysical data of the new compound are reported.
